Information card for entry 4346442

Structure parameters

• Common name: Compound 2
• Formula: C43 H52 Cl2 N2 O8 Rh2
• Calculated formula: C43 H52 Cl2 N2 O8 Rh2
• Title of publication: Axial Ligand Coordination to the C-H Amination Catalyst Rh2(esp)2: A Structural and Spectroscopic Study.
• Authors of publication: Warzecha, Evan; Berto, Timothy C.; Berry, John F.
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 17
• Pages of publication: 8817 - 8824
• a: 18.378 ± 0.0007 Å
• b: 10.4361 ± 0.0004 Å
• c: 23.1475 ± 0.0008 Å
• α: 90°
• β: 94.4895 ± 0.0015°
• γ: 90°
• Cell volume: 4425.9 ± 0.3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.028
• Residual factor for significantly intense reflections: 0.0259
• Weighted residual factors for significantly intense reflections: 0.0612
• Weighted residual factors for all reflections included in the refinement: 0.0625
• Goodness-of-fit parameter for all reflections included in the refinement: 1.115
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No