Information card for entry 4346647

Structure parameters

• Formula: C25 H55 Cl N4 Ni O2 Si
• Calculated formula: C25 H55 Cl N4 Ni O2 Si
• Title of publication: Turning a New Leaf on Metal-TMC Chemistry: Ni(II)(TMC) Acetylides.
• Authors of publication: Tyler, Sarah F.; Natoli, Sean N.; Vlaisavljevich, Bess; Fanwick, Phillip E.; Ren, Tong
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 20
• Pages of publication: 10058 - 10064
• a: 43.9611 ± 0.0017 Å
• b: 9.0601 ± 0.0004 Å
• c: 17.3189 ± 0.0007 Å
• α: 90°
• β: 111.638 ± 0.003°
• γ: 90°
• Cell volume: 6411.9 ± 0.5 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0735
• Residual factor for significantly intense reflections: 0.063
• Weighted residual factors for significantly intense reflections: 0.1798
• Weighted residual factors for all reflections included in the refinement: 0.191
• Goodness-of-fit parameter for all reflections included in the refinement: 1.105
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No