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Information card for entry 4346764
Preview
Coordinates | 4346764.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H16 Cl4 F6 Mn N3 O3 P |
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Calculated formula | C22 H16 Cl4 F6 Mn N3 O3 P |
Title of publication | Intramolecular C-C Bond Coupling of Nitriles to a Diimine Ligand in Group 7 Metal Tricarbonyl Complexes. |
Authors of publication | Yempally, Veeranna; Fan, Wai Yip; Arndtsen, Bruce A.; Bengali, Ashfaq A. |
Journal of publication | Inorganic chemistry |
Year of publication | 2015 |
Journal volume | 54 |
Journal issue | 23 |
Pages of publication | 11441 - 11449 |
a | 8.0245 ± 0.0006 Å |
b | 14.7573 ± 0.0011 Å |
c | 11.9344 ± 0.0009 Å |
α | 90° |
β | 100.46 ± 0.003° |
γ | 90° |
Cell volume | 1389.79 ± 0.18 Å3 |
Cell temperature | 105 K |
Ambient diffraction temperature | 105 K |
Number of distinct elements | 8 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0442 |
Residual factor for significantly intense reflections | 0.0432 |
Weighted residual factors for significantly intense reflections | 0.1182 |
Weighted residual factors for all reflections included in the refinement | 0.1188 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.074 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.34139 Å |
Diffraction radiation type | GaKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4346764.html
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structural data.