Information card for entry 4347453

Structure parameters

• Formula: C92 H104 Dy4 N16 O35
• Calculated formula: C92 H94 Dy4 N16 O35
• Title of publication: Lanthanide-Directed Fabrication of Four Tetranuclear Quadruple Stranded Helicates Showing Magnetic Refrigeration and Slow Magnetic Relaxation.
• Authors of publication: Mondal, Amit Kumar; Jena, Himanshu Sekhar; Malviya, Amita; Konar, Sanjit
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 11
• Pages of publication: 5237 - 5244
• a: 17.336 ± 0.003 Å
• b: 17.945 ± 0.003 Å
• c: 18.528 ± 0.003 Å
• α: 108.258 ± 0.005°
• β: 94.285 ± 0.005°
• γ: 90.647 ± 0.005°
• Cell volume: 5454.8 ± 1.6 ų
• Cell temperature: 106 ± 2 K
• Ambient diffraction temperature: 105.7 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1039
• Residual factor for significantly intense reflections: 0.0882
• Weighted residual factors for significantly intense reflections: 0.1964
• Weighted residual factors for all reflections included in the refinement: 0.2176
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0951
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No