Information card for entry 4347817

Structure parameters

• Formula: C42 H37 N7 O4 Os P
• Calculated formula: C42 H37 N7 O4 Os P
• SMILES: [Os]1(Oc2c(c3oc4c([n]13)cccc4)cccc2)([NH]=C(N)NO)(C#N)(C#N)C#N.[P+](c1ccccc1)(c1ccccc1)(c1ccccc1)c1ccccc1.OC
• Title of publication: Aerobic Oxidation of an Osmium(III) N-Hydroxyguanidine Complex To Give Nitric Oxide.
• Authors of publication: Xiang, Jing; Wang, Qian; Yiu, Shek-Man; Man, Wai-Lun; Kwong, Hoi-Ki; Lau, Tai-Chu
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 10
• Pages of publication: 5056 - 5061
• a: 10.3167 ± 0.0002 Å
• b: 12.3418 ± 0.0003 Å
• c: 15.883 ± 0.0004 Å
• α: 99.22 ± 0.002°
• β: 90.675 ± 0.002°
• γ: 101.913 ± 0.002°
• Cell volume: 1951.1 ± 0.08 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0253
• Residual factor for significantly intense reflections: 0.0231
• Weighted residual factors for significantly intense reflections: 0.0586
• Weighted residual factors for all reflections included in the refinement: 0.0593
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No