Information card for entry 4348138

Structure parameters

• Formula: C16 H19 N5 O8 V2
• Calculated formula: C16 H19 N5 O8 V2
• SMILES: [V]12(Oc3ccccc3C=[N]1NC1O[V]3(Oc4c(C=[N]3[N]2=1)cccc4)(=O)=O)(=O)=O.OC.[NH4+]
• Title of publication: Vanadium(V) Complexes with Substituted 1,5-bis(2-hydroxybenzaldehyde)carbohydrazones and Their Use As Catalyst Precursors in Oxidation of Cyclohexane.
• Authors of publication: Dragancea, Diana; Talmaci, Natalia; Shova, Sergiu; Novitchi, Ghenadie; Darvasiová, Denisa; Rapta, Peter; Breza, Martin; Galanski, Markus; Kož\?íšek, Jozef; Martins, Nuno M. R.; Martins, Luísa M D R S; Pombeiro, Armando J. L.; Arion, Vladimir B.
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 18
• Pages of publication: 9187 - 9203
• a: 9.1328 ± 0.0007 Å
• b: 10.9497 ± 0.0008 Å
• c: 11.179 ± 0.0007 Å
• α: 65.847 ± 0.007°
• β: 84.709 ± 0.006°
• γ: 74.717 ± 0.007°
• Cell volume: 983.82 ± 0.14 ų
• Cell temperature: 173 ± 0.14 K
• Ambient diffraction temperature: 173 ± 0.14 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0803
• Residual factor for significantly intense reflections: 0.0519
• Weighted residual factors for significantly intense reflections: 0.0839
• Weighted residual factors for all reflections included in the refinement: 0.0963
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No