Information card for entry 4348208

Structure parameters

• Formula: C54 H58 N12 Ni2 O17
• Calculated formula: C54 H58 N12 Ni2 O17
• Title of publication: Syntheses, X-ray structures, catalytic activity and magnetic properties of two new coordination polymers of Co(ii) and Ni(ii) based on benzenedicarboxylate and linear N,N′-donor Schiff base linkers
• Authors of publication: Bhattacharya, Biswajit; Maity, Dilip Kumar; Pachfule, Pradip; Colacio, Enrique; Ghoshal, Debajyoti
• Journal of publication: Inorg. Chem. Front.
• Year of publication: 2014
• Journal volume: 1
• Journal issue: 5
• Pages of publication: 414
• a: 19.6754 ± 0.0003 Å
• b: 11.3812 ± 0.0003 Å
• c: 27.5363 ± 0.0005 Å
• α: 90°
• β: 107.342 ± 0.001°
• γ: 90°
• Cell volume: 5885.9 ± 0.2 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0482
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for significantly intense reflections: 0.1246
• Weighted residual factors for all reflections included in the refinement: 0.128
• Goodness-of-fit parameter for all reflections included in the refinement: 1.122
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No