Information card for entry 4348637

Structure parameters

• Common name: (PPN)2Si(NO3)6
• Formula: C72 H60 N8 O18 P4 Si
• Calculated formula: C72 H60 N8 O18 P4 Si
• Title of publication: Homoleptic Poly(nitrato) Complexes of Group 14 Stable at Ambient Conditions.
• Authors of publication: Portius, Peter; Peerless, Benjamin; Davis, Martin; Campbell, Rory
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 17
• Pages of publication: 8976 - 8984
• a: 13.1566 ± 0.0005 Å
• b: 15.5873 ± 0.0006 Å
• c: 17.2414 ± 0.0008 Å
• α: 85.964 ± 0.002°
• β: 77.737 ± 0.002°
• γ: 83.246 ± 0.002°
• Cell volume: 3427.4 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1004
• Residual factor for significantly intense reflections: 0.0512
• Weighted residual factors for significantly intense reflections: 0.0909
• Weighted residual factors for all reflections included in the refinement: 0.108
• Goodness-of-fit parameter for all reflections included in the refinement: 0.957
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No