Information card for entry 4349027

Structure parameters

• Formula: C20 H48 Ag4 B48 Cl44 N8
• Calculated formula: C20 H48 Ag4 B48 Cl44 N8
• Title of publication: Chlorination of 1-Carba-closo-dodecaborate and 1-Ammonio-closo-dodecaborate Anions.
• Authors of publication: Saleh, Mahmoud; Powell, Douglas R.; Wehmschulte, Rudolf J.
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 20
• Pages of publication: 10617 - 10627
• a: 19.978 ± 0.002 Å
• b: 29.28 ± 0.004 Å
• c: 18.961 ± 0.002 Å
• α: 90°
• β: 118.716 ± 0.002°
• γ: 90°
• Cell volume: 9727.2 ± 1.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0302
• Residual factor for significantly intense reflections: 0.0258
• Weighted residual factors for significantly intense reflections: 0.0607
• Weighted residual factors for all reflections included in the refinement: 0.0634
• Goodness-of-fit parameter for all reflections included in the refinement: 0.984
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No