Information card for entry 4349366

Structure parameters

• Formula: C43.5 H79 K O7.5 Os P2
• Calculated formula: C43.5 H79 K O7.5 Os P2
• Title of publication: mer, fac, and Bidentate Coordination of an Alkyl-POP Ligand in the Chemistry of Nonclassical Osmium Hydrides.
• Authors of publication: Esteruelas, Miguel A.; García-Yebra, Cristina; Martín, Jaime; Oñate, Enrique
• Journal of publication: Inorganic chemistry
• Year of publication: 2017
• Journal volume: 56
• Journal issue: 1
• Pages of publication: 676 - 683
• a: 17.0875 ± 0.0009 Å
• b: 15.2536 ± 0.0008 Å
• c: 19.5724 ± 0.001 Å
• α: 90°
• β: 109.627 ± 0.001°
• γ: 90°
• Cell volume: 4805.1 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0549
• Residual factor for significantly intense reflections: 0.0386
• Weighted residual factors for significantly intense reflections: 0.0857
• Weighted residual factors for all reflections included in the refinement: 0.0946
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No