Information card for entry 4349706

Structure parameters

• Formula: C21 H74 Gd N19 O24 P4
• Calculated formula: C21 H50 Gd N19 O24 P4
• Title of publication: Stoichiometry of lanthanide(iii) complexes with tripodal aminophosphonic ligands ‒ a new solution to an old problem
• Authors of publication: Janicki, Rafał; Gałęzowska, Joanna; Mondry, Anna
• Journal of publication: Inorganic Chemistry Frontiers
• Year of publication: 2017
• Journal volume: 4
• Journal issue: 7
• Pages of publication: 1200
• a: 11.9496 ± 0.0006 Å
• b: 14.1528 ± 0.0007 Å
• c: 16.1651 ± 0.0009 Å
• α: 105.71 ± 0.005°
• β: 94.36 ± 0.004°
• γ: 90.901 ± 0.004°
• Cell volume: 2622.2 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.188
• Residual factor for significantly intense reflections: 0.1014
• Weighted residual factors for significantly intense reflections: 0.1484
• Weighted residual factors for all reflections included in the refinement: 0.1839
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No