Crystallography Open Database

Information card for entry 4350261

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Coordinates	4350261.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H20 N P
Calculated formula	C21 H20 N P
Title of publication	Scope and limitations of the base-catalyzed phospha-peterson P=C bond-forming reaction.
Authors of publication	Yam, Mandy; Chong, Jonathan H.; Tsang, Chi-Wing; Patrick, Brian O.; Lam, Anita E.; Gates, Derek P.
Journal of publication	Inorganic chemistry
Year of publication	2006
Journal volume	45
Journal issue	13
Pages of publication	5225 - 5234
a	11.0156 ± 0.0012 Å
b	17.2536 ± 0.0016 Å
c	9.4749 ± 0.001 Å
α	90°
β	107.886 ± 0.005°
γ	90°
Cell volume	1713.8 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0673
Residual factor for significantly intense reflections	0.0427
Weighted residual factors for significantly intense reflections	0.1122
Weighted residual factors for all reflections included in the refinement	0.1244
Goodness-of-fit parameter for all reflections included in the refinement	1.054
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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