Information card for entry 4350386

Structure parameters

• Common name: complex 10 (Maldonado) [(TpFu,MeZn)2(OH)](ClO4)
• Chemical name: Bis(hydrotris(3-(2’-furyl)-5-methylpyrazol-1-yl)borate zinc) hydroxyde
• Formula: C48 H45 B2 Cl N12 O11 Zn2
• Calculated formula: C48 H44 B2 Cl N12 O10.99 Zn2
• Title of publication: Zn-OH2 and Zn-OH complexes with hydroborate-derived tripod ligands: a comprehensive study.
• Authors of publication: Ibrahim, Mohamed M.; Olmo, Cristina Pérez; Tekeste, Teame; Seebacher, Jan; He, Guosen; Maldonado Calvo, José A; Böhmerle, Karin; Steinfeld, Gunther; Brombacher, Horst; Vahrenkamp, Heinrich
• Journal of publication: Inorganic chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 18
• Pages of publication: 7493 - 7502
• a: 11.786 ± 0.002 Å
• b: 11.786 ± 0.002 Å
• c: 31.507 ± 0.008 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 3790.3 ± 1.3 ų
• Cell temperature: 247 ± 2 K
• Ambient diffraction temperature: 247 ± 2 K
• Number of distinct elements: 7
• Space group number: 146
• Hermann-Mauguin space group symbol: R 3 :H
• Hall space group symbol: R 3
• Residual factor for all reflections: 0.095
• Residual factor for significantly intense reflections: 0.0576
• Weighted residual factors for significantly intense reflections: 0.1462
• Weighted residual factors for all reflections included in the refinement: 0.1816
• Goodness-of-fit parameter for all reflections included in the refinement: 1.129
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No