Information card for entry 4350442

Structure parameters

• Common name: TcCl4(thioxane)2*thioxane
• Chemical name: tetrachlorobis(thioxane)technetium(IV) thioxane solvate
• Formula: C12 H24 Cl4 O3 S3 Tc
• Calculated formula: C12 H24 Cl4 O3 S3 Tc
• Title of publication: Technetium tetrachloride as a precursor for small technetium(IV) complexes.
• Authors of publication: Hagenbach, Adelheid; Yegen, Eda; Abram, Ulrich
• Journal of publication: Inorganic chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 18
• Pages of publication: 7331 - 7338
• a: 6.47 ± 0.001 Å
• b: 6.469 ± 0.001 Å
• c: 12.831 ± 0.003 Å
• α: 93.95 ± 0.02°
• β: 93.87 ± 0.02°
• γ: 104.46 ± 0.02°
• Cell volume: 516.79 ± 0.17 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0709
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for significantly intense reflections: 0.0941
• Weighted residual factors for all reflections included in the refinement: 0.1046
• Goodness-of-fit parameter for all reflections included in the refinement: 0.796
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No