Crystallography Open Database

Information card for entry 4500542

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Coordinates	4500542.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H22 O11 Pb2
Calculated formula	C20 H22 O11 Pb2
Title of publication	Two Unprecedented Three-Dimensional PbIIPolymorphs and Structural Diversities Built on a Kinked Flexible Dicarboxylate Building Block
Authors of publication	Yang, Guo-Ping; Hou, Lei; Wang, Yao-Yu; Zhang, Ya-Nan; Shi, Qi-Zhen; Batten, Stuart R.
Journal of publication	Crystal Growth & Design
Year of publication	2011
Journal volume	11
Journal issue	4
Pages of publication	936
a	9.1296 ± 0.0008 Å
b	10.226 ± 0.0009 Å
c	13.0963 ± 0.0011 Å
α	103.408 ± 0.001°
β	90.242 ± 0.001°
γ	99.456 ± 0.001°
Cell volume	1172.03 ± 0.18 Å³
Cell temperature	273 ± 2 K
Ambient diffraction temperature	273 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0452
Residual factor for significantly intense reflections	0.0318
Weighted residual factors for significantly intense reflections	0.0753
Weighted residual factors for all reflections included in the refinement	0.0784
Goodness-of-fit parameter for all reflections included in the refinement	1.011
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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