Information card for entry 4501403

Structure parameters

• Formula: C46 H50 N14 O4 Sm W
• Calculated formula: C46 H50 N14 O4 Sm W
• Title of publication: Syntheses, Structures, and Magnetic Properties of Five Novel Octacyanometallate-Based Lanthanide Complexes with Helical Chains
• Authors of publication: Qian, Su-Yan; Zhou, Hu; Yuan, Ai-Hua; Song, You
• Journal of publication: Crystal Growth & Design
• Year of publication: 2011
• Journal volume: 11
• Journal issue: 12
• Pages of publication: 5676
• a: 15.289 ± 0.0015 Å
• b: 20.5 ± 0.0016 Å
• c: 21.715 ± 0.0012 Å
• α: 90°
• β: 123.397 ± 0.003°
• γ: 90°
• Cell volume: 5682.2 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0783
• Residual factor for significantly intense reflections: 0.0532
• Weighted residual factors for significantly intense reflections: 0.1148
• Weighted residual factors for all reflections included in the refinement: 0.1211
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No