Crystallography Open Database

Information card for entry 4501549

Preview

Coordinates	4501549.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C68 H32 F24 N0 O18 Pb6
Calculated formula	C68 H32 F24 O18 Pb6
Title of publication	An Unprecedented Eight-Connected Self-Penetrating Coordination Framework Based on Cage-Shaped [Pb6(μ4-O)2(O2C)8] Clusters
Authors of publication	Li, Dong-Sheng; Wu, Ya-Pan; Zhang, Peng; Du, Miao; Zhao, Jun; Li, Cheng-Peng; Wang, Yao-Yu
Journal of publication	Crystal Growth & Design
Year of publication	2010
Journal volume	10
Journal issue	5
Pages of publication	2037
a	34.081 ± 0.002 Å
b	10.751 ± 0.0008 Å
c	23.6158 ± 0.0018 Å
α	90°
β	117.064 ± 0.001°
γ	90°
Cell volume	7705.4 ± 0.9 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0768
Residual factor for significantly intense reflections	0.0595
Weighted residual factors for significantly intense reflections	0.1419
Weighted residual factors for all reflections included in the refinement	0.1476
Goodness-of-fit parameter for all reflections included in the refinement	1.092
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4501549.html