Information card for entry 4502574

Structure parameters

• Formula: As4 H144 K7 Na6 Nd3 O212 W41
• Calculated formula: As4 K3 Na3 Nd3 O193 W41
• Title of publication: Disassembly and Reassembly of Polyoxometalates: The Formation of Chains from an Adaptable Precursor
• Authors of publication: Ritchie, Chris; Boskovic, Colette
• Journal of publication: Crystal Growth & Design
• Year of publication: 2010
• Journal volume: 10
• Journal issue: 2
• Pages of publication: 488
• a: 20.454 ± 0.003 Å
• b: 21.893 ± 0.004 Å
• c: 23.565 ± 0.004 Å
• α: 87.502 ± 0.003°
• β: 81.844 ± 0.003°
• γ: 70.296 ± 0.003°
• Cell volume: 9834 ± 3 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1302
• Residual factor for significantly intense reflections: 0.0974
• Weighted residual factors for significantly intense reflections: 0.2141
• Weighted residual factors for all reflections included in the refinement: 0.2347
• Goodness-of-fit parameter for all reflections included in the refinement: 1.11
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No