Information card for entry 4503700

Structure parameters

• Formula: C6 H26.5 F Ge7 N4.5 O17
• Calculated formula: C4 F Ge7 N3 O17
• Title of publication: SU-22 and SU-23: Layered Germanates Built from 4-Coordinated Ge7Clusters Exhibiting Structural Variations on the 44Topology
• Authors of publication: Shi, Lei; Bonneau, Charlotte; Li, Yafeng; Sun, Junliang; Yue, Huijuan; Zou, Xiaodong
• Journal of publication: Crystal Growth & Design
• Year of publication: 2008
• Journal volume: 8
• Journal issue: 10
• Pages of publication: 3695
• a: 16.0583 ± 0.0008 Å
• b: 16.4484 ± 0.001 Å
• c: 17.7788 ± 0.0008 Å
• α: 90°
• β: 98.151 ± 0.006°
• γ: 90°
• Cell volume: 4648.5 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0638
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for significantly intense reflections: 0.1053
• Weighted residual factors for all reflections included in the refinement: 0.108
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No