Information card for entry 4504670

Structure parameters

• Formula: C6 H53 N2 O99 Si2 Sm5 W22
• Calculated formula: C6 H14 N2 O99 Si2 Sm5 W22
• Title of publication: Syntheses and Structures of One- and Two-Dimensional Organic−Inorganic Hybrid Rare Earth Derivatives Based on Monovacant Keggin-Type Polyoxotungstates
• Authors of publication: Wang, Jing-Ping; Zhao, Jun-Wei; Duan, Xian-Ying; Niu, Jing-Yang
• Journal of publication: Crystal Growth & Design
• Year of publication: 2006
• Journal volume: 6
• Journal issue: 2
• Pages of publication: 507
• a: 12.894 ± 0.003 Å
• b: 13.193 ± 0.003 Å
• c: 20.591 ± 0.004 Å
• α: 108.09 ± 0.03°
• β: 90.69 ± 0.03°
• γ: 107.79 ± 0.03°
• Cell volume: 3148.2 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1031
• Residual factor for significantly intense reflections: 0.0798
• Weighted residual factors for significantly intense reflections: 0.164
• Weighted residual factors for all reflections included in the refinement: 0.1782
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No