Information card for entry 4504733

Structure parameters

• Chemical name: hexaaquobis(4,4'-bipyridine)holmium(III) heptaaquo-4,4'-bipyridineholmium(III) cobalt (III) bis(dicarbollide) hydrate 4,4-bipyridine mono-protonated 4,4-bipyridine ethanol clathrate
• Formula: C273 H525 B216 Co12 Ho3 N42 O31.5
• Calculated formula: C273 H488.5 B216 Co12 Ho3 N42 O31.5
• Title of publication: Hydrogen-Bonded 3-D Network Structures of Lanthanide Aquo Ions and 4,4‘-Bipyridine with Carbaborane Anions
• Authors of publication: Cunha-Silva, Luis; Westcott, Aleema; Whitford, Nina; Hardie, Michaele J.
• Journal of publication: Crystal Growth & Design
• Year of publication: 2006
• Journal volume: 6
• Journal issue: 3
• Pages of publication: 726
• a: 13.7506 ± 0.0013 Å
• b: 29.005 ± 0.003 Å
• c: 54.61 ± 0.005 Å
• α: 97.532 ± 0.004°
• β: 95.524 ± 0.004°
• γ: 94.95 ± 0.004°
• Cell volume: 21384 ± 4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.183
• Residual factor for significantly intense reflections: 0.1649
• Weighted residual factors for significantly intense reflections: 0.4087
• Weighted residual factors for all reflections included in the refinement: 0.4145
• Goodness-of-fit parameter for all reflections included in the refinement: 2.718
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No