Information card for entry 4506013

Structure parameters

• Formula: C24 H18 N4 O4 Zn
• Calculated formula: C24 H18 N4 O4 Zn
• Title of publication: Temperature-Dependent in Situ Reduction of 4,4′-Azobispyridine via Solvothermal Reaction
• Authors of publication: Gai, Yan-Li; Jiang, Fei-Long; Xiong, Ke-Cai; Chen, Lian; Yuan, Da-Qiang; Zhang, Lin-Jie; Zhou, Kang; Hong, Mao-Chun
• Journal of publication: Crystal Growth & Design
• Year of publication: 2012
• Journal volume: 12
• Journal issue: 4
• Pages of publication: 2079
• a: 11.775 ± 0.0018 Å
• b: 11.775 ± 0.0018 Å
• c: 15.111 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2095.1 ± 0.6 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 114
• Hermann-Mauguin space group symbol: P -4 21 c
• Hall space group symbol: P -4 2n
• Residual factor for all reflections: 0.0229
• Residual factor for significantly intense reflections: 0.0219
• Weighted residual factors for significantly intense reflections: 0.0577
• Weighted residual factors for all reflections included in the refinement: 0.0583
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No