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Information card for entry 4508075
Preview
Coordinates | 4508075.cif |
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Original paper (by DOI) | HTML |
Chemical name | cyclo-(tetrakis(2-oxo-4-methoxybenzaldehyde isonicotinylhydrazonato-O,O',N,N') tetrakis(cis-dioxo molybdenum(VI))-dichloromethane(1/2.5) |
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Formula | C30.5 H27 Cl5 Mo2 N6 O10 |
Calculated formula | C30.5 H26 Cl5 Mo2 N6 O10 |
Title of publication | Three Polymorphic Forms of a Monomeric Mo(VI) Complex: Building Blocks for Two Metal‒Organic Supramolecular Isomers. Intermolecular Interactions and Ligand Substituent Effects |
Authors of publication | Vrdoljak, Višnja; Prugovečki, Biserka; Matković-Čalogović, Dubravka; Hrenar, Tomica; Dreos, Renata; Siega, Patrizia |
Journal of publication | Crystal Growth & Design |
Year of publication | 2013 |
Journal volume | 13 |
Journal issue | 8 |
Pages of publication | 3773 |
a | 28.8951 ± 0.0007 Å |
b | 9.6243 ± 0.0002 Å |
c | 27.6282 ± 0.0006 Å |
α | 90° |
β | 90.607 ± 0.002° |
γ | 90° |
Cell volume | 7682.8 ± 0.3 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 6 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0417 |
Residual factor for significantly intense reflections | 0.034 |
Weighted residual factors for significantly intense reflections | 0.0754 |
Weighted residual factors for all reflections included in the refinement | 0.0789 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.048 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4508075.html
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