Information card for entry 4508619

Structure parameters

• Formula: C6 H44 Ge O55 S3 Sm2.5 W11
• Calculated formula: C6 H16 Ge O55 S3 Sm2.5 W11
• Title of publication: Novel Rare Earth Germanotungstates and Organic Hybrid Derivatives: Synthesis and Structures of M/[α-GeW11O39] (M = Nd, Sm, Y, Yb) and Sm/[α-GeW11O39](DMSO)
• Authors of publication: Wang, Jing-Ping; Duan, Xian-Ying; Du, Xiao-Di; Niu, Jing-Yang
• Journal of publication: Crystal Growth & Design
• Year of publication: 2006
• Journal volume: 6
• Journal issue: 10
• Pages of publication: 2266
• a: 12.8034 ± 0.0008 Å
• b: 44.52 ± 0.003 Å
• c: 11.4867 ± 0.0007 Å
• α: 90°
• β: 107.52 ± 0.001°
• γ: 90°
• Cell volume: 6243.8 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0472
• Residual factor for significantly intense reflections: 0.0416
• Weighted residual factors for significantly intense reflections: 0.0975
• Weighted residual factors for all reflections included in the refinement: 0.1001
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No