Information card for entry 4508621

Structure parameters

• Formula: C10 H49 Ge N2.5 O44.75 W11 Yb
• Calculated formula: C10 H30 Ge N2.5 O44.75 W11 Yb
• Title of publication: Novel Rare Earth Germanotungstates and Organic Hybrid Derivatives: Synthesis and Structures of M/[α-GeW11O39] (M = Nd, Sm, Y, Yb) and Sm/[α-GeW11O39](DMSO)
• Authors of publication: Wang, Jing-Ping; Duan, Xian-Ying; Du, Xiao-Di; Niu, Jing-Yang
• Journal of publication: Crystal Growth & Design
• Year of publication: 2006
• Journal volume: 6
• Journal issue: 10
• Pages of publication: 2266
• a: 27.834 ± 0.006 Å
• b: 22.706 ± 0.005 Å
• c: 23.818 ± 0.005 Å
• α: 90°
• β: 123.12 ± 0.03°
• γ: 90°
• Cell volume: 12607 ± 6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0711
• Residual factor for significantly intense reflections: 0.0585
• Weighted residual factors for significantly intense reflections: 0.1408
• Weighted residual factors for all reflections included in the refinement: 0.1476
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No