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Information card for entry 4510247
Preview
Coordinates | 4510247.cif |
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Original paper (by DOI) | HTML |
Formula | C32 H53 Cu2 Ge N8 O44.5 W12 |
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Calculated formula | C32 H44 Cu2 Ge N8 O44.5 W12 |
Title of publication | Reversible Dehydration in Polyoxometalate-Based Hybrid Compounds: A Study of Single-Crystal to Single-Crystal Transformations in Keggin-Type Germanotungstates Decorated with Copper(II) Complexes of Tetradentate N-Donor Ligands |
Authors of publication | Iturrospe, Amaia; San Felices, Leire; Reinoso, Santiago; Artetxe, Beñat; Lezama, Luis; Gutiérrez-Zorrilla, Juan M. |
Journal of publication | Crystal Growth & Design |
Year of publication | 2014 |
Journal volume | 14 |
Journal issue | 5 |
Pages of publication | 2318 |
a | 11.54269 ± 0.00008 Å |
b | 22.41402 ± 0.00014 Å |
c | 25.84917 ± 0.00016 Å |
α | 90° |
β | 102.449 ± 0.0007° |
γ | 90° |
Cell volume | 6530.4 ± 0.08 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0564 |
Residual factor for significantly intense reflections | 0.0554 |
Weighted residual factors for significantly intense reflections | 0.1447 |
Weighted residual factors for all reflections included in the refinement | 0.1456 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.132 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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