Information card for entry 4510368

Structure parameters

• Formula: C28 H20 O10 Pb4
• Calculated formula: C28 H20 O10 Pb4
• Title of publication: Helical∞1[Pb2O] Chains in Polymorphs of Pb2O(C6H5COO)2
• Authors of publication: Easterday, Clay C.; Dedon, Liv R.; Zeller, Matthias; Oertel, Catherine M.
• Journal of publication: Crystal Growth & Design
• Year of publication: 2014
• Journal volume: 14
• Journal issue: 4
• Pages of publication: 2048
• a: 31.9415 ± 0.0009 Å
• b: 36.1537 ± 0.001 Å
• c: 10.8862 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 12571.4 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.0719
• Residual factor for significantly intense reflections: 0.0378
• Weighted residual factors for significantly intense reflections: 0.0561
• Weighted residual factors for all reflections included in the refinement: 0.0635
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No