Information card for entry 4510860

Structure parameters

• Formula: C20.25 H33 K N O6.88 Os
• Calculated formula: C20.25 H33 K N O6.875 Os
• Title of publication: Os(VI)O2/K Metal‒Organic Frameworks: Infinite Chain, Grid, and Porous Networks
• Authors of publication: Eckshtain-Levi, Meital; Yufit, Dmitry; Shimon, Linda J. W.; Kirillov, Alexander M.; Benisvy, Laurent
• Journal of publication: Crystal Growth & Design
• Year of publication: 2014
• Journal volume: 14
• Journal issue: 6
• Pages of publication: 2703
• a: 34.5483 ± 0.0015 Å
• b: 10.6845 ± 0.0005 Å
• c: 27.5819 ± 0.0011 Å
• α: 90°
• β: 107.569 ± 0.002°
• γ: 90°
• Cell volume: 9706.4 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0341
• Residual factor for significantly intense reflections: 0.0257
• Weighted residual factors for significantly intense reflections: 0.0537
• Weighted residual factors for all reflections included in the refinement: 0.0563
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No