Information card for entry 4511037

Structure parameters

• Formula: C104 H62 N16 O19 Pb4
• Calculated formula: C104 H56 N16 O19 Pb4
• Title of publication: A Series of Lead(II) Complexes with π−π Stackings: Structural Diversities by Varying the Ligands
• Authors of publication: Yang, Jin; Ma, Jian-Fang; Liu, Ying-Ying; Ma, Ji-Cheng; Batten, Stuart R.
• Journal of publication: Crystal Growth & Design
• Year of publication: 2009
• Journal volume: 9
• Journal issue: 4
• Pages of publication: 1894
• a: 9.324 ± 0.0019 Å
• b: 13.562 ± 0.003 Å
• c: 18.148 ± 0.004 Å
• α: 95.33 ± 0.03°
• β: 90.47 ± 0.03°
• γ: 100.64 ± 0.03°
• Cell volume: 2244.9 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0439
• Residual factor for significantly intense reflections: 0.0314
• Weighted residual factors for significantly intense reflections: 0.0688
• Weighted residual factors for all reflections included in the refinement: 0.0732
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No