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Information card for entry 4511784
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Coordinates | 4511784.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | [HNi(PtBu2NPh2)](BF4) |
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Formula | C148 H222 B3 F12 N14 Ni3 P12 |
Calculated formula | C148 H222 B3 F12 N14 Ni3 P12 |
Title of publication | Catalytic Oxidation of Alcohol via Nickel Phosphine Complexes with Pendant Amines |
Authors of publication | Weiss, Charles J.; Das, Parthapratim; Miller, Deanna L.; Helm, Monte L.; Appel, Aaron M. |
Journal of publication | ACS Catalysis |
Year of publication | 2014 |
Journal volume | 4 |
Journal issue | 9 |
Pages of publication | 2951 |
a | 14.8297 ± 0.0008 Å |
b | 11.6379 ± 0.0006 Å |
c | 43.244 ± 0.002 Å |
α | 90° |
β | 92.88 ± 0.002° |
γ | 90° |
Cell volume | 7453.9 ± 0.7 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 7 |
Space group number | 13 |
Hermann-Mauguin space group symbol | P 1 2/n 1 |
Hall space group symbol | -P 2yac |
Residual factor for all reflections | 0.0691 |
Residual factor for significantly intense reflections | 0.0405 |
Weighted residual factors for significantly intense reflections | 0.0805 |
Weighted residual factors for all reflections included in the refinement | 0.0903 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.011 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4511784.html
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