Information card for entry 4512160

Structure parameters

• Formula: C8 H120 K4 Na16 O148 Tb4 W20
• Calculated formula: C8 K4 Na16 O148 Tb4 W20
• Title of publication: Rectangle versus Square Oxalate-Connective Tetralanthanide Cluster Anchored in Lacunary Lindqvist Isopolytungstates: Syntheses, Structures, and Properties
• Authors of publication: Zhao, Junwei; Li, Hailou; Li, Yanzhou; Li, Chunyang; Wang, Zhenling; Chen, Lijuan
• Journal of publication: Crystal Growth & Design
• Year of publication: 2014
• Journal volume: 14
• Journal issue: 11
• Pages of publication: 5495
• a: 10.015 ± 0.007 Å
• b: 19.598 ± 0.013 Å
• c: 19.64 ± 0.014 Å
• α: 106.185 ± 0.01°
• β: 92.996 ± 0.011°
• γ: 95.207 ± 0.011°
• Cell volume: 3675 ± 4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0891
• Residual factor for significantly intense reflections: 0.0612
• Weighted residual factors for significantly intense reflections: 0.1482
• Weighted residual factors for all reflections included in the refinement: 0.1615
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No