Information card for entry 4513275

Structure parameters

• Common name: 1666 bm AgClO4-eggcrate squeezed
• Chemical name: Silver perchlorate / 4-[di(pyrazol-1-yl)methyl]pyridine / hexamethylene- teramine 3:3:1 coordination polymer, 2-dimensional, with unknown solvent squeezed and not contained in chemical formula and quantities derived thereof.
• Formula: C42 H45 Ag3 Cl3 N19 O12
• Calculated formula: C42 H45 Ag3 Cl3 N19 O12
• Title of publication: Robust 2D Coordination Networks from a Two-Step Assembly Process with Predesigned Silver Cyclic Dimers and Hexamethylenetetramine
• Authors of publication: Durá, Gema; Carrión, M. Carmen; Jalón, Félix A.; Manzano, Blanca R.; Rodríguez, Ana M.; Mereiter, Kurt
• Journal of publication: Crystal Growth & Design
• Year of publication: 2015
• Journal volume: 15
• Journal issue: 7
• Pages of publication: 3321
• a: 22.5686 ± 0.0005 Å
• b: 22.5686 ± 0.0005 Å
• c: 22.2724 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 9824.4 ± 0.4 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 6
• Space group number: 166
• Hermann-Mauguin space group symbol: R -3 m :H
• Hall space group symbol: -R 3 2"
• Residual factor for all reflections: 0.0843
• Residual factor for significantly intense reflections: 0.064
• Weighted residual factors for significantly intense reflections: 0.2089
• Weighted residual factors for all reflections included in the refinement: 0.2277
• Goodness-of-fit parameter for all reflections included in the refinement: 1.124
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No