Information card for entry 4513625

Structure parameters

• Formula: K2 Na6 Si46
• Calculated formula: K4.188 Na3.812 Si46
• Title of publication: Crystal Growth through Field-Assisted Electrochemical Redox and Ion-Exchange Reactions: A Case Study of K4.2Na3.8Si46Clathrate-I
• Authors of publication: Dong, Yongkwan; Nolas, George S.
• Journal of publication: Crystal Growth & Design
• Year of publication: 2015
• Journal volume: 15
• Journal issue: 10
• Pages of publication: 4731
• a: 10.2296 ± 0.0004 Å
• b: 10.2296 ± 0.0004 Å
• c: 10.2296 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1070.47 ± 0.07 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 3
• Space group number: 223
• Hermann-Mauguin space group symbol: P m -3 n
• Hall space group symbol: -P 4n 2 3
• Residual factor for all reflections: 0.0181
• Residual factor for significantly intense reflections: 0.0181
• Weighted residual factors for significantly intense reflections: 0.0503
• Weighted residual factors for all reflections included in the refinement: 0.0503
• Goodness-of-fit parameter for all reflections included in the refinement: 1.362
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No