Information card for entry 4514024

Structure parameters

• Formula: C94 H118 Ge2 N2 O Si2
• Calculated formula: C94 H118 Ge2 N2 O Si2
• Title of publication: Efficient Reduction of Carbon Dioxide to Methanol Equivalents Catalyzed by Two-Coordinate Amido‒Germanium(II) and −Tin(II) Hydride Complexes
• Authors of publication: Hadlington, Terrance J.; Kefalidis, Christos E.; Maron, Laurent; Jones, Cameron
• Journal of publication: ACS Catalysis
• Year of publication: 2017
• Journal volume: 7
• Journal issue: 3
• Pages of publication: 1853
• a: 24.283 ± 0.005 Å
• b: 21.152 ± 0.004 Å
• c: 17.759 ± 0.004 Å
• α: 90°
• β: 114.38 ± 0.03°
• γ: 90°
• Cell volume: 8308 ± 4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.086
• Residual factor for significantly intense reflections: 0.0695
• Weighted residual factors for significantly intense reflections: 0.196
• Weighted residual factors for all reflections included in the refinement: 0.2107
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.7108 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No