Information card for entry 4514278

Structure parameters

• Formula: Cu2 Gd4 H104 O120 W19 Zn3
• Calculated formula: Cu2 Gd4 O120 W19 Zn3
• Title of publication: Structural Transformation of Porous Polyoxometalate Frameworks and Highly Efficient Biomimetic Aerobic Oxidation of Aliphatic Alcohols
• Authors of publication: Zhao, Min; Zhang, Xian-Wei; Wu, Chuan-De
• Journal of publication: ACS Catalysis
• Year of publication: 2017
• Journal volume: 7
• Journal issue: 10
• Pages of publication: 6573
• a: 16.3885 ± 0.0003 Å
• b: 16.597 ± 0.0003 Å
• c: 21.2038 ± 0.0005 Å
• α: 91.749 ± 0.002°
• β: 101.863 ± 0.002°
• γ: 113.393 ± 0.002°
• Cell volume: 5139.8 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0651
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.0924
• Weighted residual factors for all reflections included in the refinement: 0.1032
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No