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Information card for entry 4514765
Preview
Coordinates | 4514765.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H21 O3 P |
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Calculated formula | C24 H21 O3 P |
SMILES | P([C@H]1[C@H]2O[C@H](c3c2cc2OCCOc2c3)C1)(c1ccccc1)c1ccccc1 |
Title of publication | Asymmetric Hydrophosphination of Heterobicyclic Alkenes: Facile Access to Phosphine Ligands for Asymmetric Catalysis |
Authors of publication | Lu, Zhiwu; Zhang, Haoyang; Yang, Zhiping; Ding, Ning; Meng, Ling; Wang, Jun |
Journal of publication | ACS Catalysis |
Year of publication | 2019 |
Journal volume | 9 |
Journal issue | 2 |
Pages of publication | 1457 |
a | 9.561 ± 0.004 Å |
b | 9.713 ± 0.003 Å |
c | 20.717 ± 0.009 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1923.9 ± 1.3 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.036 |
Residual factor for significantly intense reflections | 0.0332 |
Weighted residual factors for significantly intense reflections | 0.0777 |
Weighted residual factors for all reflections included in the refinement | 0.0789 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.091 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4514765.html
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