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Information card for entry 4514772
Preview
Coordinates | 4514772.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C35 H54 Cl2 N2 O1.5 Zn |
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Calculated formula | C35 H54 Cl2 N2 O1.5 Zn |
Title of publication | Low-Coordinate NHC‒Zinc Hydride Complexes Catalyze Alkyne C‒H Borylation and Hydroboration Using Pinacolborane |
Authors of publication | Procter, Richard J.; Uzelac, Marina; Cid, Jessica; Rushworth, Philip J.; Ingleson, Michael J. |
Journal of publication | ACS Catalysis |
Year of publication | 2019 |
Journal volume | 9 |
Journal issue | 6 |
Pages of publication | 5760 |
a | 12.9149 ± 0.0009 Å |
b | 19.5194 ± 0.0006 Å |
c | 19.2829 ± 0.0013 Å |
α | 90° |
β | 133.379 ± 0.012° |
γ | 90° |
Cell volume | 3533.1 ± 0.8 Å3 |
Cell temperature | 150.03 ± 0.1 K |
Ambient diffraction temperature | 150.03 ± 0.1 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0736 |
Residual factor for significantly intense reflections | 0.0467 |
Weighted residual factors for significantly intense reflections | 0.0894 |
Weighted residual factors for all reflections included in the refinement | 0.1012 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.035 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4514772.html
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Users of the data should acknowledge the original authors of the
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