Three-Component Cascade Reaction of 1,1-Enediamines, <i>N</i>,<i>N</i>-Dimethylformamide Dimethyl Acetal, and 1,3-Dicarbonyl Compounds: Selective Synthesis of Diverse 2-Aminopyridine Derivatives.
Authors of publication
Zi, Quan-Xing; Yan, Sheng-Jiao; Yang, Chang-Long; Li, Kun; Lin, Jun
Journal of publication
ACS omega
Year of publication
2019
Journal volume
4
Journal issue
2
Pages of publication
2863 - 2873
a
9.4051 ± 0.0012 Å
b
9.1919 ± 0.0011 Å
c
18.885 ± 0.002 Å
α
90°
β
90.699 ± 0.002°
γ
90°
Cell volume
1632.5 ± 0.3 Å3
Cell temperature
296.15 K
Ambient diffraction temperature
296.15 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0798
Residual factor for significantly intense reflections
0.053
Weighted residual factors for significantly intense reflections
0.1405
Weighted residual factors for all reflections included in the refinement
0.1623
Goodness-of-fit parameter for all reflections included in the refinement
