Information card for entry 4515714

Structure parameters

• Formula: C27 H14 Al F16 N4
• Calculated formula: C27 H14 Al F16 N4
• Title of publication: Switchable C‒H Silylation of Indoles Catalyzed by a Thermally Induced Frustrated Lewis Pair
• Authors of publication: Han, Yuxi; Zhang, Sutao; He, Jianghua; Zhang, Yuetao
• Journal of publication: ACS Catalysis
• Year of publication: 2018
• Journal volume: 8
• Journal issue: 9
• Pages of publication: 8765
• a: 10.4075 ± 0.001 Å
• b: 10.6369 ± 0.001 Å
• c: 13.0972 ± 0.0012 Å
• α: 79.781 ± 0.002°
• β: 79.01 ± 0.002°
• γ: 71.612 ± 0.002°
• Cell volume: 1339.9 ± 0.2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0493
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for significantly intense reflections: 0.1297
• Weighted residual factors for all reflections included in the refinement: 0.1398
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No