Crystallography Open Database

Information card for entry 4516064

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Coordinates	4516064.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C45 H55 F15 N3 Nb O3
Calculated formula	C45 H55 F15 N3 Nb O3
Title of publication	Synthesis of (Arylmido)niobium(V) Complexes Containing Ketimide, Phenoxide Ligands, and Some Reactions with Phenols and Alcohols.
Authors of publication	Srisupap, Natta; Wised, Kritdikul; Tsutsumi, Ken; Nomura, Kotohiro
Journal of publication	ACS omega
Year of publication	2018
Journal volume	3
Journal issue	6
Pages of publication	6166 - 6181
a	11.3778 ± 0.0005 Å
b	12.9307 ± 0.0005 Å
c	18.995 ± 0.0006 Å
α	86.879 ± 0.003°
β	81.525 ± 0.003°
γ	77.672 ± 0.003°
Cell volume	2699.58 ± 0.18 Å³
Cell temperature	93 K
Ambient diffraction temperature	93 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0723
Residual factor for significantly intense reflections	0.0643
Weighted residual factors for significantly intense reflections	0.1972
Weighted residual factors for all reflections included in the refinement	0.2013
Goodness-of-fit parameter for all reflections included in the refinement	1.043
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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