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Information card for entry 4516253
Preview
Coordinates | 4516253.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | Ox_5j |
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Formula | C49.5 H69 Br Cl2 N O3 P Pd |
Calculated formula | C49.5 H69 Br Cl2 N O3 P Pd |
Title of publication | Pd-Catalyzed Cross-Coupling Reactions Promoted by Biaryl Phosphorinane Ligands |
Authors of publication | Laffoon, Summer D.; Chan, Vincent S.; Fickes, Michael G.; Kotecki, Brian; Ickes, Andrew R.; Henle, Jeremy; Napolitano, José G.; Franczyk, Thaddeus S.; Dunn, Travis B.; Barnes, David M.; Haight, Anthony R.; Henry, Rodger F.; Shekhar, Shashank |
Journal of publication | ACS Catalysis |
Year of publication | 2019 |
Pages of publication | 11691 |
a | 27.66 ± 0.013 Å |
b | 21.676 ± 0.01 Å |
c | 19.545 ± 0.009 Å |
α | 90° |
β | 123.911 ± 0.005° |
γ | 90° |
Cell volume | 9725 ± 8 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 8 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0612 |
Residual factor for significantly intense reflections | 0.0384 |
Weighted residual factors for significantly intense reflections | 0.0856 |
Weighted residual factors for all reflections included in the refinement | 0.095 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.006 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4516253.html
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Users of the data should acknowledge the original authors of the
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