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Information card for entry 4516256
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Coordinates | 4516256.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | Cpx_5f |
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Formula | C48 H71 F3 N O6 P Pd S |
Calculated formula | C48 H71 F3 N O6 P Pd S |
Title of publication | Pd-Catalyzed Cross-Coupling Reactions Promoted by Biaryl Phosphorinane Ligands |
Authors of publication | Laffoon, Summer D.; Chan, Vincent S.; Fickes, Michael G.; Kotecki, Brian; Ickes, Andrew R.; Henle, Jeremy; Napolitano, José G.; Franczyk, Thaddeus S.; Dunn, Travis B.; Barnes, David M.; Haight, Anthony R.; Henry, Rodger F.; Shekhar, Shashank |
Journal of publication | ACS Catalysis |
Year of publication | 2019 |
Pages of publication | 11691 |
a | 28.3488 ± 0.0004 Å |
b | 18.5998 ± 0.0003 Å |
c | 19.6316 ± 0.0003 Å |
α | 90° |
β | 112.701 ± 0.001° |
γ | 90° |
Cell volume | 9549.5 ± 0.3 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 8 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0416 |
Residual factor for significantly intense reflections | 0.0364 |
Weighted residual factors for significantly intense reflections | 0.1267 |
Weighted residual factors for all reflections included in the refinement | 0.1339 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.155 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4516256.html
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