Information card for entry 4517218

Structure parameters

• Formula: C20 H40 O4 S Si4
• Calculated formula: C20 H40 O4 S Si4
• SMILES: S(=O)(=O)(c1ccc(C(C[Si]([Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C)C(=O)OC)cc1)C
• Title of publication: Arylsilylation of Electron-Deficient Alkenes via Cooperative Photoredox and Nickel Catalysis
• Authors of publication: Zhang, Zhikun; Hu, Xile
• Journal of publication: ACS Catalysis
• Year of publication: 2019
• Journal volume: 10
• Journal issue: 1
• Pages of publication: 777
• a: 22.0893 ± 0.0004 Å
• b: 9.47947 ± 0.00015 Å
• c: 14.2315 ± 0.0003 Å
• α: 90°
• β: 107.915 ± 0.002°
• γ: 90°
• Cell volume: 2835.51 ± 0.1 ų
• Cell temperature: 140 ± 0.1 K
• Ambient diffraction temperature: 140 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0428
• Residual factor for significantly intense reflections: 0.0414
• Weighted residual factors for significantly intense reflections: 0.1124
• Weighted residual factors for all reflections included in the refinement: 0.1139
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No