Crystallography Open Database

Information card for entry 4518221

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Coordinates	4518221.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H60 N24 P4 Pd4
Calculated formula	C46 H60 N24 P4 Pd4
Title of publication	Synthesis and Structure of Multinuclear Pd(II) Complexes Bridged by Phosphide or Azide Ligands.
Authors of publication	Takeuchi, Katsuhiko; Kim, Kun-Woo; Kim, Yong-Joo; Fukaya, Norihisa; Sato, Kazuhiko; Choi, Jun-Chul
Journal of publication	ACS omega
Year of publication	2020
Journal volume	5
Journal issue	46
Pages of publication	29706 - 29713
a	23.5646 ± 0.0002 Å
b	13.3084 ± 0.0001 Å
c	38.4626 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	12062.2 ± 0.17 Å³
Cell temperature	93 ± 2 K
Ambient diffraction temperature	93 ± 2 K
Number of distinct elements	5
Space group number	33
Hermann-Mauguin space group symbol	P n a 21
Hall space group symbol	P 2c -2n
Residual factor for all reflections	0.0365
Residual factor for significantly intense reflections	0.0362
Weighted residual factors for significantly intense reflections	0.0971
Weighted residual factors for all reflections included in the refinement	0.0973
Goodness-of-fit parameter for all reflections included in the refinement	1.17
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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