Information card for entry 4518426

Structure parameters

• Formula: C32 H34 O4 Si
• Calculated formula: C32 H34 O4 Si
• Title of publication: Three-Component Ni-Catalyzed Silylacylation of Alkenes
• Authors of publication: Ni, Dongshun; Brown, M. Kevin
• Journal of publication: ACS Catalysis
• Year of publication: 2021
• Pages of publication: 1858 - 1862
• a: 9.4521 ± 0.0005 Å
• b: 26.2261 ± 0.0015 Å
• c: 11.8032 ± 0.0007 Å
• α: 90°
• β: 103.62 ± 0.002°
• γ: 90°
• Cell volume: 2843.6 ± 0.3 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0837
• Residual factor for significantly intense reflections: 0.0748
• Weighted residual factors for significantly intense reflections: 0.1145
• Weighted residual factors for all reflections included in the refinement: 0.1175
• Goodness-of-fit parameter for all reflections included in the refinement: 1.272
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No