Information card for entry 4518457

Structure parameters

• Formula: C29 H53 Co P2
• Calculated formula: C29 H48 Co P2
• Title of publication: Cobalt-Hydride-Catalyzed Hydrosilylation of 3-Alkynes Accompanying π-Bond Migration
• Authors of publication: Kim, Yeong Bum; Kim, Dongwook; Dighe, Shashikant U.; Chang, Sukbok; Park, Jung-Woo
• Journal of publication: ACS Catalysis
• Year of publication: 2021
• Pages of publication: 1548 - 1553
• a: 9.289 ± 0.0019 Å
• b: 9.1 ± 0.0018 Å
• c: 16.695 ± 0.003 Å
• α: 90°
• β: 91.33 ± 0.03°
• γ: 90°
• Cell volume: 1410.8 ± 0.5 ų
• Cell temperature: 243 ± 2 K
• Ambient diffraction temperature: 243 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0901
• Residual factor for significantly intense reflections: 0.0664
• Weighted residual factors for significantly intense reflections: 0.1893
• Weighted residual factors for all reflections included in the refinement: 0.2104
• Goodness-of-fit parameter for all reflections included in the refinement: 1.15
• Diffraction radiation wavelength: 0.73 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No