Information card for entry 4518566
| Formula |
C18 H25 Cl N3 Ni P |
| Calculated formula |
C18 H25 Cl N3 Ni P |
| Title of publication |
Redox-Neutral Imination of Alcohol with Azide: A Sustainable Alternative to the Staudinger/Aza-Wittig Reaction |
| Authors of publication |
Li, Huaifeng; Lupp, Daniel; Das, Pradip K.; Yang, Li; Gonçalves, Théo P.; Huang, Mei-Hui; El Hajoui, Marwa; Liang, Lan-Chang; Huang, Kuo-Wei |
| Journal of publication |
ACS Catalysis |
| Year of publication |
2021 |
| Journal volume |
11 |
| Journal issue |
7 |
| Pages of publication |
4071 - 4076 |
| a |
16.1382 ± 0.0015 Å |
| b |
8.1442 ± 0.0008 Å |
| c |
16.0627 ± 0.0018 Å |
| α |
90° |
| β |
118.179 ± 0.003° |
| γ |
90° |
| Cell volume |
1860.9 ± 0.3 Å3 |
| Cell temperature |
120 ± 2 K |
| Ambient diffraction temperature |
119.99 K |
| Number of distinct elements |
6 |
| Space group number |
14 |
| Hermann-Mauguin space group symbol |
P 1 21/c 1 |
| Hall space group symbol |
-P 2ybc |
| Residual factor for all reflections |
0.0576 |
| Residual factor for significantly intense reflections |
0.0407 |
| Weighted residual factors for significantly intense reflections |
0.0903 |
| Weighted residual factors for all reflections included in the refinement |
0.0959 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.078 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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https://www.crystallography.net/4518566.html
