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Information card for entry 4518572
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Coordinates | 4518572.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C25 H27 N3 O3 |
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Calculated formula | C25 H27 N3 O3 |
Title of publication | Ruthenium-Catalyzed Radical Cyclization/meta-Selective C‒H Alkylation of Arenes via σ-Activation Strategy |
Authors of publication | Gou, Xue-Ya; Li, Yuke; Luan, Yu-Yong; Shi, Wei-Yu; Wang, Cui-Tian; An, Yang; Zhang, Bo-Sheng; Liang, Yong-Min |
Journal of publication | ACS Catalysis |
Year of publication | 2021 |
Journal volume | 11 |
Journal issue | 7 |
Pages of publication | 4263 - 4270 |
a | 31.7124 ± 0.0014 Å |
b | 6.29804 ± 0.00019 Å |
c | 22.6491 ± 0.0005 Å |
α | 90° |
β | 93.248 ± 0.003° |
γ | 90° |
Cell volume | 4516.3 ± 0.3 Å3 |
Cell temperature | 285.3 ± 0.4 K |
Ambient diffraction temperature | 285.3 ± 0.4 K |
Number of distinct elements | 4 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.065 |
Residual factor for significantly intense reflections | 0.0555 |
Weighted residual factors for significantly intense reflections | 0.1483 |
Weighted residual factors for all reflections included in the refinement | 0.1555 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.034 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4518572.html
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