Information card for entry 4518622
| Formula |
C22 H22 N2 O3 Pd |
| Calculated formula |
C22 H22 N2 O3 Pd |
| Title of publication |
DMPDAB‒Pd‒MAH: A Versatile Pd(0) Source for Precatalyst Formation, Reaction Screening, and Preparative-Scale Synthesis |
| Authors of publication |
Huang, Jingjun; Isaac, Matthew; Watt, Ryan; Becica, Joseph; Dennis, Emma; Saidaminov, Makhsud I.; Sabbers, William A.; Leitch, David C. |
| Journal of publication |
ACS Catalysis |
| Year of publication |
2021 |
| Pages of publication |
5636 - 5646 |
| a |
9.1137 ± 0.0009 Å |
| b |
10.222 ± 0.001 Å |
| c |
12.2985 ± 0.0012 Å |
| α |
70.989 ± 0.002° |
| β |
70.567 ± 0.002° |
| γ |
71.163 ± 0.002° |
| Cell volume |
991.53 ± 0.17 Å3 |
| Cell temperature |
100 ± 2 K |
| Ambient diffraction temperature |
99.96 K |
| Number of distinct elements |
5 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0171 |
| Residual factor for significantly intense reflections |
0.0162 |
| Weighted residual factors for significantly intense reflections |
0.0422 |
| Weighted residual factors for all reflections included in the refinement |
0.0427 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.063 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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https://www.crystallography.net/4518622.html
