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Information card for entry 4518630
Preview
Coordinates | 4518630.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C29 H26 O2 Si |
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Calculated formula | C29 H26 O2 Si |
Title of publication | Palladium-Catalyzed (4 + 4) Annulation of Silacyclobutanes and 2-Iodobiarenes to Eight-Membered Silacycles via C‒H and C‒Si Bond Activation |
Authors of publication | Zhu, Ming-Hui; Zhang, Xiao-Wen; Usman, Muhammad; Cong, Hengjiang; Liu, Wen-Bo |
Journal of publication | ACS Catalysis |
Year of publication | 2021 |
Pages of publication | 5703 - 5708 |
a | 18.71438 ± 0.0001 Å |
b | 7.11566 ± 0.00005 Å |
c | 17.68547 ± 0.00011 Å |
α | 90° |
β | 98.0756 ± 0.0005° |
γ | 90° |
Cell volume | 2331.73 ± 0.03 Å3 |
Cell temperature | 296.86 ± 0.1 K |
Ambient diffraction temperature | 296.86 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0372 |
Residual factor for significantly intense reflections | 0.0358 |
Weighted residual factors for significantly intense reflections | 0.1023 |
Weighted residual factors for all reflections included in the refinement | 0.1036 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.058 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4518630.html
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